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HEAp–SiCp/7075Al复合材料的搅拌摩擦加工制备及性能研究

Research on the Preparation and Properties of HEAp–SiCp/7075Al Composite Materials by Friction Stir Processing

  • 摘要: 采用多道次搅拌摩擦加工工艺,制备不同SiC含量的高熵合金颗粒–碳化硅颗粒增强7075铝基(HEAp–SiCp/7075Al)复合材料,研究SiC含量对其成形质量、界面特征、力学性能及摩擦磨损行为的影响,优化7075Al合金的综合性能。结果表明:SiC质量分数为2%时,增强颗粒在焊核区分散均匀,与基体界面结合致密;质量分数增至5%和10%后,颗粒团聚加剧,均匀性显著下降。显微硬度随SiC含量增加呈升高趋势,2%,5%和10%试样焊核区平均硬度分别为150.97,160.96,163.71 HV。拉伸性能变化规律则与之相反,2%试样极限抗拉强度最优,达416.5 MPa,归因于高含量下团聚加重。断口分析表明,复合材料呈韧–脆混合断裂模式,随SiC含量增加,主导机制由颗粒断裂逐渐转为界面脱黏与团聚。摩擦磨损性能随SiC含量提升而显著改善,10%试样磨痕最浅,耐磨性最佳。综上,增强颗粒的分散均匀性对力学性能调控作用显著,适量SiC与高熵合金协同增强可实现强度与耐磨性的协同优化。本研究为高熵合金颗粒增强铝基复合材料的成分优化与工艺设计提供了实验依据与理论参考。

     

    Abstract: To optimize the mechanical and tribological properties of 7075Al alloy, a multi-pass friction stir processing technique was employed to fabricate HEAp–SiCp/7075Al composites with varying SiC particle contents. The influence of SiC content on the forming quality, interfacial characteristics, mechanical properties, and tribological behavior of the composites was investigated. The results indicate that at a SiC mass fraction of 2%, the reinforcing particles are uniformly dispersed in the nugget zone and tightly bonded to the matrix interface. With increasing SiC content, agglomeration becomes more severe and dispersion uniformity decreases. Microhardness exhibits an increasing trend with SiC content, with average nugget-zone hardness values reaching 150.97 HV, 160.96 HV, and 163.71 HV for the 2%, 5%, and 10% SiC specimens, respectively. In contrast, the tensile properties show the opposite trend;the 2% SiC specimen exhibits the best ultimate tensile strength of 416.5 MPa, attributed to aggravated agglomeration at higher contents. Fracture analysis reveals a ductile-brittle mixed mode, and as the SiC content increases, the dominant fracture mechanism shifts from particle fracture to interfacial debonding and agglomeration. Tribological performance significantly improves with the increase in SiC content, with the 10% SiC specimen exhibiting the smallest wear scar depth and the best wear resistance. Overall, the uniform dispersion of reinforcing particles plays a significant role in tuning the mechanical properties, and the synergistic reinforcement of an appropriate amount of SiC and high-entropy alloy (HEA) enables a comprehensive improvement in both strength and wear resistance of the composite. These findings provide experimental evidence and theoretical guidance for the composition optimization and process design of HEA particle-reinforced aluminum matrix composites.

     

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